Advanced Structural and Functional Characterization
RESEARCH UNITS
Advanced Structural and Functional Characterization
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In the Magnetic Material and Functional Oxides department at ICMAB, the activities of the Crystallography of Magnetic and Electronic Oxides and Surfaces group are addressed to explore, understand and develop new strongly correlated materials of interest in fundamental Condensed Matter research and as novel materials for the Information technologies.
The activities of the group are based on the application of chemical and magnetic crystallography methods to the investigation of emergent functional oxides. Combining an intensive use of Large Scale Facilities (such as neutron and synchrotron sources) with symmetry analysis methodologies, we investigate the symmetry-properties relationship associated to structural, magnetic or electronic orders in functional oxides.
Current research lines include the study of structure-properties relationship in new magnetic, multiferroic and magnetoelectric materials with special charge, spin or electronic orders, and the study of novel oxides with giant responses for technological applications. In addition to bulk materials and films, surface diffraction synchrotron techniques and surface characterization methods are also applied to the study of ordering related phenomena in low-dim systems.
The neutron scattering in the field of magnetic and electronic materials presents extraordinary importance. To probe magnetic properties on atomic scale, neutron diffraction is an established technique and a unique method of choice, which allows perfect quantitative data interpretation. The magnetic moment of the neutron makes it a unique probe for magnetic properties in condensed matter on atomic scale. It gives a direct access to the spin and orbital distribution in the unit cell. In particular, magnetic structure determination is the foyer to the understanding of many fundamental phenomena in Condensed Matter research. Neutron and synchrotron techniques can be applied to investigate spin-state transitions, charge and orbital ordering, giant magneto-resistance, magnetoelectric materials as well as other emergent phenomena in frustrated materials such as spin ice, spin liquid behavior or other promising topological defects.
Multiferroics are important functional materials featuring strongly coupled order parameters that can be manipulated by external fields. Magnetoelectric multiferroics are receiving enormous attention as they open the road to new forms of multifunctional devices. However, they challenge our fundamental understanding of magnetic and ferroelectric order because a strong magnetoelectric coupling is incompatible with traditional mechanisms of ferroelectricity. The recent discovery of a new class of materials (type-II multiferroics) in which the magnetic and electric properties are strongly coupled is attracting very much interest because of the possibility to manipulate magnetism and spins by electric fields and vice-versa, to magnetically control electric charges. Future applications in information technology require new multiferroic materials fulfilling all technological requirements. Along with its technological functionalities, multiferroics are also of great interest in fundamental research into strongly correlated oxides and quantum matter.
Cobalt oxides present a plethora of very interesting properties like metal-insulator transitions, spin-state changes, giant magnetoresistance, double-exchange, phase separation, high thermoelectric power, oxygen diffusivity, mixed-conduction, charge and orbital ordering or superconductivity among others. These properties are interesting not only from a fundamental point of view but also due to their potential applicability in different fields. One very remarkable characteristic of many cobalt compounds is the ability of Co ions to adopt different spin states. This makes that Co oxides have, in comparison with other transition metal oxides, an extra degree of freedom: the spin state of Co. So, the investigation of novel cobaltites with different structures and prepared in different forms is between the most attractive opportunities within strongly correlated systems: the spin state of Co at selected sites in the structure plays a key role in the structural, magnetic, magnetotransport properties, electronic and ion mobility or the thermoelectric power. This research is inscribed inside the wider objective of understand and control the spin state and electronics degrees of freedom of Co cations, especially with 3+ valence. Trivalent cobalt oxides exhibit unique electronic phases characterized by the interplay between nearly degenerate spin states.
The Functional Surfaces and Interfaces Research Unit is formed by two Research Groups: the Functional Nanomaterials and Surfaces (FunNanoSurf) group and the Physical Chemistry of Surfaces and Interfaces (Surfaces) group.
Both groups have in common the study at the nanoscale of structural and electronic properties of nanostructures, surfaces and interfaces.
The FunNanoSurf group focuses more on molecular-based, supramolecular and polymeric aggregates.
The Surfaces group on the synthesis, characterization and manipulation of organic semiconductor surfaces and interfaces.
The Molecular Materials for Electronic Devices (eMolMat) group is focused on the design and synthesis/preparation of new functional molecular materials for their application in organic/molecular electronic devices. This is an interdisciplinary group where researchers from different disciplines (i.e., chemistry, materials science, physics, engineering, etc.) are working together. Our work ranges from fundamental studies in order to better understand materials properties to a more applied perspective aiming at developing proof-of-principle devices.
Particularly, our areas of interest include synthesis of novel functional molecules (electroactive molecules, organic radicals, etc.), surface self-assembly, crystal engineering, molecular switches, organic field-effect transistors (OFETs) and electrolyte-gated field-effect transistors (EGOFETs), charge transport and organic-based (bio)-sensors.
Ramon y Cajal Researcher
Postdoctoral Researcher
The main scientific topics of the group are related to the preparation and characterization of novel organic molecular materials and their application in molecular electronic devices.
In particular, our interests include:
The Nanostructured Materials for Optoelectronics and Energy Harvesting Research Unit is formed by two Research Groups that focus their activities on materials for energy applications: the Nanostructured Materials for Optoelectronics and Energy Harvesting (NANOPTO) group and the Laser Processing (LASER) group.
The NANOPTO group studies the synthesis, characterization and application of semiconducting structures for organic and perovskite photovoltaics, organic thermoelectrics, and photonics.
The LASER group is focused on the preparation of nanostructures functional materials using multiple laser techniques.
The Smart Molecular Inorganic and Hybrid Materials Research Unit is formed by two groups who work especially with inorganic chemistry for biomedical applications, among others: the Inorganic Materials and Catalysis (LMI) group, and the Nanoparticles and Nanocomposites (NN) group.
The LMI group studies the synthesis, preparation and characterization of boron-based compounds, such as carboranes, borane clusters and MOFs, for energy and biomedical applications, such as BNCT for cancer treatment.
The NN group focuses its research in the synthesis and characterization of small inorganic nanoparticles or thin films for information technology or biomedical applications, and studies the interaction between these elements and the biological systems, such as cells or the model organism C. elegans.
The Solid State Chemistry (SSC) Research Unit is formed by an interdisciplinary Research Group with the same name that focuses on solid state transformations and processes that lead to new inorganic, polymeric, nanocarbon and nanostructured hybrid materials with direct applications in energy, electronics and biomedicine. The group has the following Research Lines: Electrochemistry and electroactive materials; Supercritical Fluids and Functional Materials; Nitride-Based Materials; Inorganic Materials for Battery Applications; Nanoengineering of Carbon and Inorganic Materials and Nanostructured interfaces for electrochemical energy storage.
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The Superconducting Materials and Large Scale Nanostructures (SUMAN) Research Unit is formed by a Research Group with the same name that focuses on the synthesis, preparation and characterization of high-temperature superconducting materials. The idea is to find low-cost processes to be able to scale up the production of this kind of materials and make them competitive for power applications.
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The group interests relate to the fields of nanoscience and nanotechnology, particularly the areas of molecular electronics, molecular magnetism and biology. We design molecular systems capable of providing inputs at the nano-scale and focus our efforts in the control and organization of such species on different surfaces/nanodevices.
The main areas of expertise are
A main project in the group is the creation of advanced molecular systems that can be accomodated (hence, be inserted) within graphene electrodes toward the creation of robust hybrid three-terminal nanodevices. My view involves the synthesis of the desired molecules (curcuminoid (CCMoids)/porphyrinoid (PPDS) in nature), their characterization in bulk (solid state and studies in solution) and deposition on graphene electrodes. In a first stage such systems can act as nano-wires, capable exclusively of electronic transport however, coordination of such systems to metallic centers can provide additional propertie highly interesting in spintronics toward the creation of switches and memory nanodevices.
Our goal is the control of the properties and study of deposition of such molecules having as a final step the I-V measurements of the final nanodevices. With this in mind, we collaborate with international groups (STM, MCBJ and BJ techniques) and perform the measurements ourselves by the use of a cryogenic probe station.
This project is linked to an ERC-consolidator Grant (Acronym: Tmol4TRANS).
A major aim of crystal engineering and supramolecular chemistry is the rational synthesis of metallo-aggregates and self-assembled systems with new functions based on novel magnetic properties, light responsiveness, biomedical applications, catalytic activity, fluorescence, or redox properties, among others. These useful and interesting properties may lead to the application of such assemblies, as for example: in sensors, compact information storage devices for next-generation computers, catalysts in industrial processes and medical applications (such as implants, contrast agents for CAT scans,…).
The goal here is the design, synthesis and characterization, with a strong emphasis on the material properties, of these novel species. This approach involves the specific combination of polydentate ligands (curcuminoid (CCMoids)/porphyrinoid (PPDS)) that can accommodate a number of metallic/metalloid centers, providing interesting optic and/or electronic features. Additional bridging ligands may also be used to facilitate the creation of different architectures (1D (chains), 2D (layers) and 3D (MOFs, coordination polymers).
Considering this major aim, our projects include detailed spectroscopic characterizations of the final species by advanced techniques (SQUID, EPR, NMR, electrochemistry, fluorecence studies, …) as well as deposition in different surfaces/electrodes (functionalized or not, Au, graphene, Si/SiO2, using different techniques as for example µ-CP, micro-contact printing) of the final species, then studies of the created substrates (AFM, TEM, SEM, STM, XPS,…) and electronic/optical final properties (creation of three-terminal devices, confocal microscopy, etc).
Closely related to nanotechnology, many promising advanced materials are based on magnetic principles. At the nanoscale such features can be related to the paramagnetic behavior of coordination compounds (0D). Therefore, a most challenging project is the development of organic-inorganic hybrid materials, with emphasis in such property.
Here, I am interested in develop materials with 3d/4f centers with emphasis in the control of coordination of such systems, their magnetic characterization and nano-structuration. Regarding the last part, coordination molecules are soft-materials and it is crucial to determine the optimal deposition method/s toward the creation of robust systems.
The design, characterization and study of properties of such systems are closely related to the techniques described in the other lines. Overall. the three lines unify in the general idea of making functional materials based on molecules taking advantages on the properties of the organic ligand (curcuminoid (CCMoids)/ porphyrinoid (PPDS)) and/or the metallic center.
Focused on unraveling and controlling the nanoscale structural and electronic properties of nanostructures and interfaces through surface engineering. Devoting special effort to organic materials, part of our investigation centers on organic semiconductors with relevance as active layers for electronic devices (such as organic solar cells and organic field effect transistors).
Our research spans from fundamental issues in organic growth to the electronic response of metal-organic junctions within two main research activities:
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Research group focused on the development and integration of new materials, basically nanometric oxide thin films, and the exploration of their use in photovoltaics, electronics, spintronics, data storage and computing. These broad and scientifically challenging objectives are currently major social demands, as silicon-based electronics is reaching its limit in size, speed and efficiency, and radically new approaches, energy sustainable, are needed.
Specifically, current activities include
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ICREA Research Professor – UAB
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The group focuses on producing and characterizing advanced semiconducting structures with the main objective of understanding their fundamental behavior in order to tailor and improve their functionalities and empower different applications in the areas of optoelectronics, energy-related, and sensing devices.
The group is divided into 4 different research activities:
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NANOMOL-BIO is devoted to the synthesis, physico-chemical characterization and development, up to pre-clinical regulatory phases, of molecular and polymeric (nano)materials for biomedical applications:
Molecular Materials for Therapy:
Molecular Materials for Diagnosis:
Research Scientist
Director of Nanomol-TECNIO
Principal Investigator of Nanomol at CIBER-BBN
Head of the Nanomol-Bio Group
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Emeritus Research Professor
Ramon y Cajal Researcher and Max Planck Partner Grup Leader
CIBER- Postdoctoral Researcher
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The Molecular Nanoscience and Organic Materials (NANOMOL) Research Unit focuses on the study, synthesis and processing of molecular and polymeric materials with biomedical, electronic, magnetic and chemical properties.
NANOMOL is composed by two research groups: “Molecular Materials for Electronic Devices” (e-MolMat) and "Nanostructured Molecular Materials for Biomedicines" (NANOMOL-BIO).
eMolMat is focused on the design and synthesis of organic molecules and materials for their integration in electronic devices such as memories, switches, transistors or sensors. Both fundamental studies and proof-of-concept devices are pursued.
NANOMOL-BIO is devoted to the synthesis, physico-chemical characterization and development, up to pre-clinical regulatory phases, of molecular and polymeric (nano)materials for biomedical applications: (i) biomolecule and small molecule delivery, (ii) diagnosis, (iii) regenerative medicine and (iv) immunotherapy.
NANOMOL is member of the Biomedical Research Network (CIBER) in the area of Bioengineering, Biomaterials and Nanomedicine; and is awarded with the TECNIO label given to Catalan research groups with high innovative and tech transfer capacities.
The Thermal Analysis and Surface Area Analysis Service is used for the study of the behavior of materials when temperature changes under different conditions and atmospheres, and for studies of surface area and porosity. The Service allows for simultaneous thermogravimetric analysis (TGA- DSC/DTA), differential scanning calorimetry (DSC), as well as Brunauer–Emmett–Teller (BET) Surface Area Analysis.
Thermal Analysis Technician
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BET Surface Area Analysis Technician
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The Thermal Analysis Service of ICMAB includes two equipments, a simultaneous thermogravimetric analysis (TG)- differential scanning calorimetry/differential thermal analysis (heat flow DSC /DTA) system NETZSCH -STA 449 F1 Jupiter, and a differential scanning calorimeter (power compensation DSC) Perkin Elmer DSC8500 LAB SYS (N5340501) equipped with a Liquid N2 controller CRYOFILL (N534004)
To request this service, please fill the application form in the link left and leave it together with the sample in the closet located at in the ground floor. For further information please contact the service technician Roberta Ceravola This email address is being protected from spambots. You need JavaScript enabled to view it.
Thermal Analysis Laboratory
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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By phone:
+34 935801853
Ext. 270
IMB-CNM-CSIC
ICN2-CSIC
UAB
Molecular Beam
Epitaxy
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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By phone:
+34 935801853
Ext. 281
Technical support
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Spectrophotometer Jasco 4700. Energy range: 300-7800 cm-1. The Service is provided with a Attenuated Total Reflectance accessory (ATR) for powder samples, films, polymers, liquids, etc. Powder samples can also be measured making KBr pellets.
This equipment is of self-service management for internal users, who have been previously trained by the technicians. However, the technicians are needed for the external users
There are two double beam UV-Vis-NIR spectrophotometer, a by Jasco V-780 and a Jasco V-770 with operational range of 190-3300 nm and also a Shimadzu UV-Vis 1700 spectrophotometer with operational range of 200-800 nm.
Liquid samples can be measured in absorbance or transmittance mode mainly using 1 cm or 1 mm quartz cuvettes. The three equipments are of self-service management for internal users, who have been previously trained by the technicians. However, the technicians are needed for the external users.
For solid samples it is available a Diffuse Reflectance Sphere DRA-2500 accessory in the UV-Vis-NIR Jasco V-770 spectrophotometer, with operational range of 190-3300 nm. Solid samples can be measured mainly in reflectance or transmittance mode.
A qualified technician is always needed for running the DRA-2500 accessory.
INTERNAL USERS
First contact with the Service Technicians Vega Lloveras (This email address is being protected from spambots. You need JavaScript enabled to view it., ext. 300, 311). They will train the users to manage the equipment by themselves because it works in a self-service regime for internal users.
All users must register in the database registration of the equipment every time they use it, pointing out the time they have spent doing the measurement, the group's IP and the project's number.
EXTERNAL USERS
First contact with the Service Technicians Vega Lloveras (This email address is being protected from spambots. You need JavaScript enabled to view it., ext. 300, 311) in order to arrange the details of the measurements. At the same time, a service form must be filled in. Every equipment has its own service form. There exists the possibility of working with the apparatus in a self-service regime.
In addition to this, all users must also register in the database of the equipment every time they use it.
Follow the general procedure
1. Liquid measurements.
Follow the general procedure.
2. Solid measurements using Diffuse Reflectance Sphere (DRA-2500) accessory.
The technicians are always needed for running the DRA-2500 accessory, for internal as well as for external users. Contact with them (This email address is being protected from spambots. You need JavaScript enabled to view it., ext. 300, 311) in order to arrange the details of the measurements.
At the same time, a service form must be filled in.
In addition to this, all users must also register in the database of the equipment every time they use it.
First contact with the Service Technician Vega Lloveras (This email address is being protected from spambots. You need JavaScript enabled to view it., ext. 300, 311) in order to arrange the details of the measurements. At the same time, a service form must be filled in.
Contact with Prof. Narcís Mestres (This email address is being protected from spambots. You need JavaScript enabled to view it., ext. 227)
Spectroscopic Techniques Laboratory
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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By phone:
+34 935801853
Ext. 436100
The Service of Thin Films has been created to offer to the researchers the capability of fabrication of complex oxides thin films and heterostructures combining oxides and metals.
The deposition techniques are pulsed laser deposition (PLD) for oxides and sputtering for metals. Currently there are two PLD set-ups installed, and in short time both systems will be connected to a chamber with several sputtering units. PLD is a physical vapour deposition technique that uses ultraviolet laser radiation to vaporize material that is transferred to the substrate. The plot in Figure 1 is a sketch illustrating a PLD set-up.
Technician
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Technician
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Tel. 93 580 18 53 (ext. 303)
The technique is very suitable for oxides, and compared with other techniques is particularly useful to obtain films with complex stoichiometry and to grow epitaxial films and heterostructures. Moreover, PLD is highly versatile to optimize the deposition conditions of new materials, and the films can be grown in relatively fast processes. These characteristics favour the use of the technique by research groups having interest in different materials.
The pulsed beam of an ultraviolet laser (usually an excimer) is focused on a ceramic target placed in a vacuum chamber. The combination of pulsed irradiation, high photon energy, and high energy density can cause the ablation of the material. Ablation refers to the etching and emission of material under conditions totally out of the equilibrium. The plasma created expands fast along the perpendicular direction of the target (see the photography in Figure 2). A substrate is placed front the target, and inert or reactive gases are usually introduced during the deposition process.
Scientific Manager
Technician
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Tel. 935801853 (ext. 323-262)
Thin Films Laboratory
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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By phone:
+34 935801853
Ext. 323-262
Dr. Arevik Musheghyan (Postdoctoral contract)
Dr. Chinwe Nwanya (Women for Africa Programme, University of Nigeria)
Mr. Pablo García Lebière (PhD, ICMAB - UAB)
Mr. Gerard Felipo i Esteve (Degree final project - UAB)
Mr. Roger Garreta Piñol (Degree final project - UAB)
Ms. Emma Poupard (Internship, Polytech Nantes)
Mr. Colin Duchassouy (Internship, Centrale Lille Institut)
Dr. Yasmín Esqueda (Postdoc, CICESE, México)
Mr. Pablo García Lebière (PhD, ICMAB - UAB)
Mr. Alifhers Salim Mestra (PhD stay - PUCV, Chile)
Mr. Carlos García (Degree final project - UAB)
Mr. Roger Morales (Degree final project - UAB)
Mr. Faïz Attoumani (Internship, Polytech Nantes)
Ms. Blanca Gilabert López (Joves i Ciencia, F. Catalunya - La Pedrera)
Mr. Nick Toledo García (Internship, UB)
Ms. Anna Pérez Serrano (Internship, UB)
Mr. Alexandre Pinsach Gelabert (Internship, UB)
Mr. Gerard Felipo i Esteve (Degree final project - UAB)
Matrix Assisted Pulsed Laser Evaporation of hybrid nanocomposites
Laser Direct Write of nanostructured systems
Advanced nanomaterials for energy and environmental applications
"Laser processing of graphene and related materials for energy storage: State of the art and future prospects"
R. Kumar, A. Pérez del Pino, S. Sahoo, R. K. Singh, W. K. Tan, K. K. Kar, A. Matsuda, E. Joanni
Progress in Energy and Combustion Science 91 (2022) 100981 .
"Unravelling the origin of the capacitance in nanostructured nitrogen-doped carbon - NiO hybrid electrodes deposited with laser"
P. García Lebière, E. György, C. Logofatu, D. Naumenko, H. Amenitsch, P. Rajak, R. Ciancio, A. Pérez del Pino
Ceramics International 48 (2022) 15877.
"Meteorite controlled ablation under low vacuum studied using emission spectroscopy: a technique to sample the bulk composition of asteroids"
J. M. Trigo-Rodriguez, A. Pérez del Pino, E. Peña-Asensio, A. Rimola.
52nd Lunar and Planetary Science Conference 2021. p. 1384
"Laser synthesis of NixZnyO/reduced graphene oxide/carbon nanotube electrodes for energy storage applications"
P. García Lebière, A. Pérez del Pino, C. Logofatu, E. György
Applied Surface Science 563 (2021) 150234
"Boost of Charge Storage Performance of Graphene Nanowall Electrodes by Laser-Induced Crystallization of Metal Oxide Nanostructures"
Y. Esqueda-Barrón, A. Pérez del Pino, P. García Lebière, A. Musheghyan-Avetisyan, E. Bertran-Serra, E. György, C. Logofatu
ACS Appl. Mater. Interfaces 13 (2021) 17957−17970
"Laser fabrication of hybrid electrodes composed of nanocarbons mixed with cerium and manganese oxides for supercapacitive energy storage"
P. García Lebière, A. Pérez del Pino, G. Domènech Domingo, C. Logofatu, I. Martínez-Rovira, I. Yousef, E. György
Journal of Materials Chemistry A 9 (2021) 1192
"Deposition and Growth of Functional Nanomaterials by LDW and MAPLE Techniques"
A. Pérez del Pino
Crystals 10 (2020) 1066
"Laser synthesis of TiO2–carbon nanomaterial layers with enhanced photodegradation efficiency towards antibiotics and dyes"
R. Ivan, A. Pérez del Pino, I. Yousef, C. Logofatu, E. György
Journal of Photochemistry & Photobiology A: Chemistry 399 (2020) 112616
"New fabrication method for producing reduced graphene oxide flexible electrodes by using low-power visible laser diode engraving system"
A. Chuquitarqui, L. C. Cotet, M. Baia, E. Gyorgy, K. Magyari, L. Barbu-Tudoran, L. Baia, M. Díaz-González, C. Fernandez Sanchez, A. Perez del Pino
Nanotechnology 31 (2020) 325402
"Enhanced UV-Vis Photodegradation of Nanocomposite Reduced Graphene Oxide/Ferrite Nanofiber Films Prepared by Laser-Assisted Evaporation"
A.Queraltó, E.György, R.Ivan, A.Pérez del Pino, R.Frohnhoven, S. Mathur
Crystals 10 (2020) 271
"Carbon–based nanomaterials and ZnO ternary compound layers grown by laser technique for environmental and energy storage applications"
R.Ivan, C.Popescu, A.Pérez del Pino, C.Logofatu, E. György
Applied Surface Science 509 (2020) 145359
"Laser-induced synthesis and photocatalytic properties of hybrid organic-inorganic composite layers"
R. Ivan, C. Popescu, A. Pérez del Pino, I. Yousef, C. Logofatu, E. György
Journal of Materials Science 54 (2019) 3927–3941
"Enhancement of supercapacitive properties of laser deposited graphene-based electrodes through carbon nanotube loading and nitrogen doping"
A. Pérez del Pino, M. Rodríguez López, M. A. Ramadan, P. García Lebière, C. Logofatu, I. Martínez-Rovira, I. Yousef, E. György
Physical Chemistry Chemical Physics 21 (2019) 25175 - 25186
"A review on synthesis of graphene, h-BN and MoS2 for energy storage applications: Recent progress and perspectives"
R. Kumar, S Sahoo, E. Joanni, R K Singh, R. M. Yadav, R. K. Verma, D. P. Singh, A. Pérez del Pino, S. A. Moshkalev
Nano Research 12 (2019) 2655–2694
"Mineralization-inspired synthesis of magnetic zeolitic imidazole framework composites"
M. Hoop, A. Terzopoulou, X. Z. Chen, A. M. Hirt, M. Charilaou, Y. Shen, F. Mushtaq, A. Pérez del Pino, C. Logofatu, L. Simonelli, A. J. deMello, P. Falcaro, C. J. Doonan, B. J. Nelson, J. Puigmartí-Luis, S. Pané
Angewandte Chemie 131 (2019) 13684–13689
E. György, C. Logofatu, A. Pérez del Pino, A. Datcu, O. Pascu, R. Ivan
Ceramics International 44 (2018) 1826-1835
"Ultrafast Epitaxial Growth of Functional Oxide Thin Films by Pulsed Laser Annealing of Chemical Solutions"
A. Queraltó, A. Perez del Pino, M. de la Mata, J. Arbiol, M. Tristany, X. Obradors, T. Puig
Chemistry of Materials 28 (2016) 6136-6145.
"Titanium oxide – reduced graphene oxide – silver composite layers synthesized by laser technique: wetting and electrical properties"
E. György, A. Perez del Pino, A. Datcu, L. Duta, C. Logofatu, I. Iordache, A.Duta
Ceramics International 42 (2016) 16191–16197.
"Laser-induced Chemical Transformation of Free-standing Graphene Oxide Membranes in Liquid and Gas Ammonia Environments"
A. Pérez del Pino, E. György, C. Cotet, L. Baia, C. Logofatu
RSC Advances 6 (2016) 50034.
"Direct multipulse laser processing of titanium oxide – graphene oxide nanocomposite thin films"
A. Pérez del Pino, A. Datcu, E. György
Ceramics International 42 (2016) 7278–7283.
"Ultraviolet pulsed laser crystallization of Ba0.8Sr0.2TiO3 films on LaNiO3-coated silicon substrates"
A. Queraltó, A. Pérez del Pino, M. de la Mata, M. Tristany, X. Obradors, T. Puig, S. Trolier-McKinstry
Ceramics International 42 (2016) 4039-4047.
"Growth of ferroelectric Ba0.8Sr0.2TiO3 epitaxial films by UV pulsed laser irradiation of chemical solution derived precursor layers"
A. Queraltó, A. Pérez del Pino, M. de la Mata, J. Arbiol, M. Tristany, A. Gómez, X. Obradors, T. Puig
Applied Physics Letters 106 (2015) 262903.
"One-step preparation of nitrogen doped titanium oxide / Au / reduced graphene oxide composite thin films for photocatalytic applications"
A. Datcu, L. Duta, A. Pérez del Pino, C. Logofatu, C. Luculescu, A. Duta, E. György
RSC Advances 5 (2015) 49771.
"Laser-induced chemical transformation of graphene oxide – iron oxide nanoparticles composites deposited on polymer substrates"
A. Pérez del Pino, E. György, C. Logofatu, J. Puigmartí-Luis, W. Gao
Carbon 93 (2015) 373-383.
"Ultrafast crystallization of Ce0.9Zr0.1O2-y epitaxial films on flexible technical substrates by pulsed laser irradiation of chemical solution derived precursor layers"
A. Queraltó, A. Perez del Pino, M. de la Mata, J. Arbiol, X. Obradors, T. Puig.
Crystal Growth & Design 15 (2015) 1957-1967.
"Wetting and photoactive properties of laser irradiated zinc oxide – graphene oxide nanocomposite layers"
A. Datcu, A. Pérez del Pino, C. Logofatu, A. Duta, E. György
2015 - NATO Science for Peace and Security Series A-Chemistry and Biology, 119-125.
"Resonant Infrared and Ultraviolet Matrix Assisted Pulsed Laser Evaporation of Titanium Oxide / Graphene Oxide Composites: A Comparative Study"
S. M. O’Malley, J. Tomko, A. Pérez del Pino, C. Logofatu, E. György
The Journal of Physical Chemistry C 118 (2014) 27911-27919.
"Simultaneous Laser-Induced Reduction and Nitrogen Doping of Graphene Oxide in Titanium Oxide / Graphene Oxide Composites"
E. György, A. Pérez del Pino, C. Logofatu, C. Cazan, A. Duta
Journal of the American Ceramic Society 97 (2014) 2718.
"Wetting and photoactive properties of laser processed zinc oxide - graphene oxide nanocomposite thin layers"
E. György, A. Pérez del Pino, C. Logofatu, A. Duta
Journal of Applied Physics 116 (2014) 024906.
"Ultraviolet pulsed laser irradiation of multi-walled carbon nanotubes in nitrogen atmosphere"
A. Pérez del Pino, E. György, B. Ballesteros, L. Cabana, G. Tobias
Journal of Applied Physics 115 (2014) 093501.
"Localized template growth of functional nanofibers from an amino acid-supported framework in a microfluidic chip"
J. Puigmartí-Luis, M. Rubio-Martínez, I. Imaz, B. Z. Cvetković, L. Abad, F. J. del Campo, A. Pérez del Pino, D. Maspoch, D. B. Amabilino
ACS Nano 8 (2014) 818-826
"Study of the deposition of graphene oxide sheets by matrix assisted pulsed laser evaporation"
A. Pérez del Pino, E. György, C. Logofatu, A. Duta
Journal of Physics D: Applied Physics 46 (2013) 505309.
"Effect of laser radiation on multi-wall carbon nanotubes: study of shell structure and immobilization process"
E. György, A. Pérez del Pino, J. Roqueta, B. Ballesteros, L. Cabana, G. Tobias
Journal of Nanoparticles Research 15 (2013) 1852.
"Laser-induced metal organic decomposition for doped CeO2 epitaxial thin film growth"
A. Queraltó, A. Pérez del Pino, S. Ricart, X. Obradors, T. Puig
Journal of Alloys and Compounds 574 (2013) 246-254.
"Processing and immobilization of chondroitin-4-sulphate by UV laser radiation"
E. György, A. Pérez del Pino, J. Roqueta,A.S. Miguel, C. Maycock, A. G. Oliva
Colloids and Surfaces B: Biointerfaces 104 (2013) 169-173.
"Laser processing and immobilisation of CdSe/ZnS core-shell quantum dots"
E. György, J. Roqueta, B. Ballesteros, A. Pérez del Pino, A.S. Miguel, C. Maycock, A. G. Oliva
Physica Status Solidi A 11 (2012) 2201-2207
"Deposition of Functionalized Single Wall Carbon Nanotubes through Matrix Assisted Pulsed Laser Evaporation"
A. Pérez del Pino, E. György, L. Cabana, B. Ballesteros, G. Tobias
Carbon 50 (2012) 4450 - 4458
"Polycarbonate films metalized with a single component molecular conductor suited to strain and stress sensing applications"
E. Laukhina, Lebeded, V. Laukhin, A. Pérez del Pino, E. B. Lopes, A. I.S. Neves, D. Belo, M. Almeida, J. Veciana, C. Rovira
Organic Electronics 13 (2012) 894-898
"Synthesis and characterization of Ag nanoparticles and Ag loaded TiO2 photocatalysts"
G. Sauthier, A. Pérez del Pino, A. Figueras, E. György
Journal of American Ceramic Society 94 (2011) 3780
"Synthesis and laser immobilisation onto solid substrates of CdSe/ZnS core-shell quantum dots"
E. György, A. Pérez del Pino, J. Roqueta, B. Ballesteros, A.S. Miguel, C. Maycock, A. G. Oliva
Journal of Physical Chemistry C 115 (2011) 15210
"Effects of Pulsed Laser Radiation on Epitaxial Self-assembled Ge Quantum Dots Grown on Si Substrates"
A. Pérez del Pino, E. György, I. C. Marcus, J. Roqueta, M. I. Alonso
Nanotechnology 22 (2011) 295304
"Processing and immobilization of Ribonuclease A through laser irradiation"
C. Popescu, J. Roqueta, A. Pérez del Pino, M. Moussaoui, M. V. Nogués, E. Gyorgy
Journal of Materials Research 26 (2011) 815
"Guided Assembly of Metal and Hybrid Conductive Probes Using Floating Potential Dielectrophoresis"
Josep Puigmartí-Luis, Johannes Stadler, Daniel Schaffhauser, Ángel Pérez del Pino, Brian R. Burgcand Petra S. Dittrich
Nanoscale 3 (2011) 937-940
"Boosting electrical conductivity in a gel-derived material by nanostructuring with trace carbon nanotubes"
D. Canevet, A. Pérez del Pino, D. B. Amabilino, M. Sallé
Nanoscale 3 (2011) 2898-2902
"Nanocomposites combining conducting and superparamagnetic components prepared via an organogel"
E. Taboada, L. N. Feldborg, A. Pérez del Pino, A. Roig, D. B. Amabilino, J. Puigmartí-Luis
Soft Matter 7 (2011) 2755-2761
"Tunable optical and electrical properties of pulsed laser deposited WO3 and Ag-WO3 nanocomposite thin films"
E. Gyorgy, A. Pérez del Pino
Journal of Materials Science 46 (2011) 3560
The SPM Lab offers 2.300 hours yearly of SPM related experiments to people inside and outside the ICMAB, without including maintenance, development of new equipment, setups, calibration and implementation of new modes.
The ICMAB groups who use the service are:
Superconducting Materials & Large Scale
Nanostructured Molecular Nanoscience and Organic Materials (NANOMOL)
Multifunctional Oxides and Complex Structures
Molecular Chirality
Surfaces and Nanomaterials
These groups make up 65% of the work done by the service. To a lesser extent, the service is also used by the following groups Nanoparticles and Nanocomposites, Inorganic Materials and Catalysis and Optoelectronic Nanostructured Materials. Besides ICMAB groups, service groups performs measurements of the Institute of Microelectronics of Barcelona (Micro & Nano Tools group, Integrated Circuits and Systems (ICAS), Department of Micro i Nanosistemes. Grup Biosensors & BioMEMs) groups the Autonomous University of Barcelona (Sensors and Biosensors Group, Department of Chemistry, Reliability of electronic devices and circuits) as well as to outside companies such as Henkel (Chemical sector) or Kostal (automotive sector). In total, more than 60 different users ICMAB and 13 have used the SPM external service over the past two years.
We also carry on outreach activities inside the ICMAB that brought international attention.
Training personnel (mainly PhD) in the AFM technique is another part of the tasks done at the lab.
Technician
This email address is being protected from spambots. You need JavaScript enabled to view it.
Tel. +34 935801853 Ext. 388
Technician
This email address is being protected from spambots. You need JavaScript enabled to view it.
Tel. +34 935801853 Ext. 388
Keysight 5100 AFM comprises a scanner of 60 x 60 microns in X / Y and 6 microns in the Z axis. The equipment can use a special liquid cell and controlled environment chamber for conducting scanners at low humidity or in nitrogen. The maximum sample size is 3x3 cm in X / Y and 2 cm thick. The equipment works in the Constant Amplitude Dynamic mode for obtaining topographic images, however Contact mode is also a possibility. The equipment uses an external generator module that can apply in-plane magnetic fields upto + -800 Oe. The equipment is specifically employed to acquired topographic images, having a low noise architecture that allow the acquisition of 500 nm size images.
We offer a broad range of services, including Topography, PFM, EFM, KPFM, CSAFM, PCAFM and SThM. Send us the Request Form to get a quotation.
[18] Iglesias, L., Gómez, A., Gich, M., Rivadulla, F., (2018) . Tuning Oxygen Vacancy Diffusion through Strain in SrTiO3 Thin Films. ACS Appl. Mater. Interfaces, 2018, 10 (41), pp 35367–35373
[17] del Moral, A., González-Rosillo, J. C., Gómez, A., Puig, T., & Obradors, X. (2018). Thermoelectric stack sample cooling modification of a commercial atomic force microscopy. Ultramicroscopy. https://doi.org/10.1016/j.ultramic.2018.10.014
[16] Daniel Suarez, Eden Steven, Elena Laukhina, Andres Gomez, Anna Crespi, Narcis Mestres, Concepció Rovira, Eun Sang Choi & Jaume Veciana (2018) 2D organic molecular metallic soft material derived from BEDO-TTF with electrochromic and rectifying properties. npj Flexible Electronicsvolume 2, Article number: 29 (2018) https://doi.org/10.1038/s41528-018-0041-1
[15] Vila-Fungueiriño, J. M., Gómez, A., Antoja-Lleonart, J., Gázquez, J., Magén, C., Noheda, B., & Carretero-Genevrier, A. (2018). Direct and converse piezoelectric responses at the nanoscale from epitaxial BiFeO 3 thin films grown by polymer assisted deposition. Nanoscale. 10.1039/c8nr05737k
[14] Sandoval, S., Kepic, D., Pérez del Pino, A., Gyorgy, E., Gómez, A., Pfannmoeller, M., … & Tobias, G. (2018). Selective Laser-Assisted Synthesis of Tubular van der Waals Heterostructures of Single-Layered PbI2 within Carbon Nanotubes Exhibiting Carrier Photogeneration. ACS nano, 12(7), 6648-6656. 10.1021/acsnano.8b01638
[13] A.Gomez, T.Puig, X.Obradors, Diminish electrostatic in piezoresponse force microscopy through longer or ultra-stiff tips, Applied Surface Science
Volume 439, 1 May 2018, Pages 577-582, https://doi.org/10.1016/j.apsusc.2018.01.080
[12] A.Gomez, S.Sanchez, Mariano Campoy-Quiles, A.Abate, Topological distribution of reversible and non-reversible degradation in perovskite solar cells, Nano Energy Volume 45, March 2018, Pages 94-100, https://doi.org/10.1016/j.nanoen.2017.12.040
[11] A. Gomez, M. Gich, A. Carretero-Genevrier, T. Puig, X. Obradors, Piezo-generated charge mapping revealed through direct piezoelectric force microscopy, Nature Communicationsvolume 8, Article number: 1113 (2017) doi:10.1038/s41467-017-01361-2
[10] Alberto Quintana, Andrés Gómez, Maria Dolors Baró, Santiago Suriñach, Eva Pellicer, Jordi Sort, Self-templating faceted and spongy single-crystal ZnO nanorods: Resistive switching and enhanced piezoresponse, In Materials & Design, Volume 133, 2017, Pages 54-61, ISSN 0264-1275, https://doi.org/10.1016/j.matdes.2017.07.039.
[9] Gómez, A., Vila-Fungueiriño, J. M., Moalla, R., Saint-Girons, G., Gázquez, J., Varela, M., Bachelet, R., Gich, M., Rivadulla, F. and Carretero-Genevrier, A. (2017), Semiconducting Films: Electric and Mechanical Switching of Ferroelectric and Resistive States in Semiconducting BaTiO3–δ Films on Silicon (Small 39/2017). Small, 13: n/a. doi:10.1002/smll.201770208
[8] A Carretero‐Genevrier, R Bachelet, G Saint‐Girons, R Moalla, JM Vila‐Fungueiriño, B Rivas‐Murias, F Rivadulla, J Rodriguez‐Carvajal, A Gomez, J Gazquez, M Gich, N Mestres, Ashutosh Tiwari, Rosario A Gerhardt, Magdalena Szutkowska. Development of Epitaxial Oxide Ceramics Nanomaterials Based on Chemical Strategies on Semiconductor Platforms (2016) Advanced Ceramic Materials
[7] David Kiefer, Liyang Yu, Erik Fransson, Andrés Gómez, Daniel Primetzhofer, Aram Amassian, Mariano Campoy-Quiles, Christian Müller (2016). A Solution-Doped Polymer Semiconductor:Insulator Blend for Thermoelectrics Advanced Science
[6] Marta Riba-Moliner, Narcis Avarvari, David. B. Amabilino , Arántzazu González-Campo, and Andrés Gómez* (2016). Distinguishing between Mechanical and Electrostatic Interaction in Single Pass Multi Frequency Electrostatic Force Microscopy Measurements on a Molecular Material. Langmuir, 2016, 32 (51), pp 13593–13599, DOI: 10.1021/acs.langmuir.6b03390
[5] Marta Riba-Moliner, Andrés Gómez-Rodríguez, David B. Amabilino, Josep Puigmartí-Luis, Arántzazu González-Campo, (2016). Functional supramolecular tetrathiafulvalene-based films with mixed valences states. Polymer
[4] Oliveras-González, C., Di Meo, F., González-Campo, A., Beljonne, D., Norman, P., Simón-Sorbed, M., … & Amabilino, D. B. (2015). Bottom-up hierarchical self-assembly of chiral porphyrins through coordination and hydrogen bonds. Journal of the American Chemical Society.
[3] Bernhard Dörling, Jason D. Ryan, Matthew C. Weisenberger, Andrea Sorrentino, Ahmed El Basati, Andrés Gomez, Miquel Garriga, Eva Pereiro, John E. Anthony, Alejandro R. Goñi, Christian Müller*, Mariano Campoy-Quiles* (2015) Photoinduced p- to n-type switching in thermoelectric polymer-carbon nanotube composites – Advanced Materials 10.1002/adma.201505521
[2] A. Queraltó, A. Pérez del Pino, M. de la Mata, J. Arbiol, M. Tristany, A. Gómez, X. Obradors and T. Puig (2015). Growth of ferroelectric Ba0.8Sr0.2TiO3 epitaxial films by ultraviolet pulsed laser irradiation of chemical solution derived precursor layers. Applied Physics Letters 106, 262903
[1] Coll, M., Gomez, A., Mas-Marza, E., Almora, O., Garcia-Belmonte, G., Campoy-Quiles, M., & Bisquert, J. (2015). Polarization Switching and Light-Enhanced Piezoelectricity in Lead Halide Perovskites. The Journal of Physical Chemistry Letters, 6(8), 1408-1413.
Piezoresponse Phase image over the topography roughness, image acquired at low humidity environment. Sample courtesy of Joan Bisquert
Current image of a Carbon nano tube doped thermoelectric film obtained with a solid platinum tip, sample biased and at low humidity environment. The data can be used to correlate topography image with current image, obtained information on the local current distribution or compare the images with different samples, using histograms from the images. Sample courtesy of Bernhard Dörling
Scanning Probe
Microscopy
ICMAB
Campus UAB, delante de caseta de Bomberos
08193, Bellaterra
Spain
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
Many investigation lines in this institute rely on the magnetic and electric properties of the materials being investigated. Most of the characterization carried out requires the use of very precise measurement systems. In order to satisfy the intensive demand of measurements of this nature, the Low Temperature and Magnetometry Service was created.
The Low Temperature and Magnetometry Service is part of the ICMAB Scientific Technical Services Unit and its facilities are available to all the research crew of the Institute, as well as, to external users. It is devoted to the measurement of the magnetic, electric properties under specific conditions of external magnetic field and temperature.
In order to achieve the demand, the Service is equipped with two SQUID based magnetometers (Quantum Design MPMS system), devoted to magnetometry measurements and two Quantum Design PPMS systems, devoted to electrical transport measurements, as well as magnetometry measurements.
A User Commission supervises the proper operation of the Service and meets once a year in order to satisfy this supervision task as well as to take the appropriate decisions for the optimization of the Service operation.
Service Technician
bbozzo(at)icmab.es
+34 93 580 18 53 ext 436211
Profile
Service Technician
fvalles(at)icmab.es
+34 93 580 18 53 ext 436099
Profile
The MPMS-3 system is the new generation of SQUID detector based magnetometers. It offers an enchanced performance of temperature stabilization, magnetic field stability when compared to those exhibited by the MPMS-XL system. This fact reduces the measurement noise, allowing the obtention of cleaner measurements for those samples with extremelly low magnetic moment. The core system consists of a superconducting longitudinal solenoid able to generate mangetic fields up to 70kOe. The system has also able to precisely control the temperature at the sample space at any value from 2K to 400K with a stability condition of less than 0.1% of oscillation.
PPMS system is bundled with a current source and a voltmeter multiplexed to three channels that can determine the resistance of three samples quasi-simultaneously using four point measurement approach. Swithing between one sample and next is done automatically and cyclically several times per second. Option can be used for the determination of the resistivity, magnetoresistance and Hall effect of the material under study. Its speficications allow the determination of resistances ranging from mOhm to approximmately 20MOhm. Sample rotator can be used with this option.
Specifications
Current: 5nA to 5mA. DC current or square wave AC (plus/minus current)
Voltage limit: 0.1mV to 95mV
Power limit: 10nW to 1mW
AC Transport uses a waveform generator able to produce driving signals that are used by the current source to produce alternating currents. The bundled voltmeter measures the voltage and the measured signal is treated using a Lock-in based software. Hardware is multiplexed to two channels, so that two samples can be measured during the same session. Related software is prepared for measuring:
Sample rotator can be used with this option.
Specifications:
Amplitude range: 10uA to 2A
Frequency range: 10Hz to 10kHz
Voltmeter scale ranges: 40uV to 5V
With this option, PPMS can be used as a magnetometer. The option hardware provides the possibility to be used as DC extraction magnetometer or an AC Susceptometer.
Specifications:
Driving field amplitude: 0.1Oe to 15Oe
Frequency range: 10Hz to 10kHz
Working temperature range: 2K to 350K
Sensibility of DC extraction: 1e-5 emu
Sensibility of AC susceptibility: 1e-8 emu
VSM based magnetometers provide a fast and precise method for the determination of the DC magnetization of a material. An specially built sample holder that contains a heater allows to extend the working temperature up to 1000K.
Specifications:
Sensibility: 1e-6 emu
Temperature range: 2K to 300K for normal measurements, 300K to 1000K is oven sample holder is used
The measurement of the magnetic torque provides an alternate system for determining the sample magnetization. The main purpose of the magnetic torque measurement is to study the mangetic anysotropy of a material.
Due to the nature of the equipment used, restrictions apply on the type of samples that can be submitted. The service will only accept samples that are prepared following the tips explained below.
Please, contact to the Service Manager for more details
The experimental setup allows only the use of bulk samples or thin fims not larger than 1x1mm2. The desired rotation must be clearly indicated either in the sample, or by using a drawing sketch.
Only bulk or thin film samples are accepted
Output data format is, by default, comma separated values with the relevant measurement fields included. Other secondary data fields are omitted.
If requested, original or RAW data files or data in other formats can also be delivered.
PLEASE, FIND YOUR DATA AT THE FOLLOWING LOCAL NETWORK FOLDERS:
Equipment Network resource
External users or users not having access to the ICMAB local network can have their data emailed or copied to removable media upon request.
For any question about the details of the measurement, contact to the Service Technician Bernat Bozzo (This email address is being protected from spambots. You need JavaScript enabled to view it., ext 436211, Lab 0.20) or Ferran Vallès (This email address is being protected from spambots. You need JavaScript enabled to view it., ext 436208, office 0.10)
Low Temperatures and
Magnetometry Service
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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By phone:
+34 935801853
Ext. 436211
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
The Soft Materials Service provides equipment and technical assistance for the preparation and characterization of micro-and nanostructured soft molecular materials (molecular surfaces, micro- and nanoparticulate molecular materials, plastic films, dispersed systems, SAMs, etc..) with interest in different areas of application (biomedicine, electronics, energy storage and other chemical and material application areas).
These equipment and services constitute unit 6 of NANBIOSIS, the integrated infrastructure for the production and characterization of nanomaterials, biomaterials and systems in biomedicine, of CIBER-BBN and the Minimal Invasion Surgery Center Jesús Usón, which has been recognized by Spanish Government as Unique Scientific-Technological Infrastructure (ICTS).
Technician
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Tel. +34 935801853 Ext. 338
Technician
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Tel. +34 935801853 Ext. 253
In order to apply for a service, please, contact with Amable Bernabé (This email address is being protected from spambots. You need JavaScript enabled to view it.). He will contact you for arrangements
For the use of lab-scale high pressure plant and high-pressure phase analyzer please contact Dr. Nora Ventosa (This email address is being protected from spambots. You need JavaScript enabled to view it.)
Preparation and Characterization of
Soft Materials
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
This email address is being protected from spambots. You need JavaScript enabled to view it.
By phone:
+34 935801853 Ext. 338
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
The electron microscopy service was created in 2008 and is mainly dedicated to research groups of the Institute, but it can be accessible to external users as well.
The service consists of a scanning electron microscope (SEM) QUANTA FEI 200 FEG-ESEM installed in September 2008 (substituting an old PHILIPS 515 acquired in 2004 as a result of a process of reallocation between the CSIC centres CID and ICMAB) and a transmission electron microscope JEOL 1210 acquired in 1991. With the acquisition of the new SEM, the service provides ICMAB with a powerful and versatile tool capable to combine routine daily work with cutting-edge research. As a general strategy, this way the service aims at satisfying in-house the increasing demand of high-profile nanostructural characterization, thus eliminating technical limits imposed by external scientific-technical services.
To promote an efficient exploitation, the service offers: 1) Technical support given by two high-profiled (doctor) staff members. 2) Electronic management. 3) Effective user-training system by technical staff, oriented to achieve a maximum degree of self-service.
Technical supervisor
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+ 34 935 801 853 (233-342)
Technical supervisor
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+ 34 935 801 853(296-344)
The Quanta 200 ESEM FEG from FEI is a special and advanced type of high performance scanning electron microscope (SEM). The FEI Quanta 200 FEG is a state of the art field emission microscope that allows nanometer level inspection of materials.
The 120 KV JEOL 1210 TEM features a high angular range (Tilt X= ± 60o, Tilt Y= ± 30o) providing a unique facility in the area of Barcelona for exploring large volumes of the reciprocal lattice by electron diffraction. It has technical support by a high profile (Dr) staff member. With a resolution below 3.2 Å this equipment is useful for low resolution structure imaging and characterization of nanoparticulate systems.
contact with the service technician, Judith Oró (This email address is being protected from spambots. You need JavaScript enabled to view it.)
RESULTS: \\Jungle\tem
Electron Microscopy
Service
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
This email address is being protected from spambots. You need JavaScript enabled to view it.
This email address is being protected from spambots. You need JavaScript enabled to view it.
By phone:
+34 935801853
Ext. 233-342 (SEM) 296-344(TEM)
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
SCIENTIFIC & TECHNICAL SERVICES
The X-ray Diffraction Laboratory is a consolidated service of the ICMAB institute. The main objective of the service is to meet the needs of the different departments of the center offering the maximum possible benefits to the institute users and it is also available to external users.
Based on the principles of X-ray diffraction, a wealth of structural and microstructural information about crystalline materials can be derived. In materials science, knowledge of the structure and composition of the materials studied is a key requirement for understanding their properties.
Our fast, accurate and customized services include data collection, qualitative and quantitative phase analysis as well as texture measurements (pole figures), residual stress, reciprocal space maps, etc. The most common function of the service is the acquisition of X-ray diffraction data under different conditions, e.g. by using flat sample and Bragg-Brentano geometry, thin film diffraction, texture determination on layers, microdiffraction and qualitative analysis in capillary materials.
Technician
Technician
Technician
The Siemens D-5000 is a powder diffractometer well suited for the analysis of powder samples and qualitative analysis.
This unit is equipped with a centric Eulerian cradle and a VANTEC-500 area detector. This combination gives the Bruker D8 the capability to handle tasks such as phase identification and quantification, textural and residual stress analysis, determination of particle size, percent crystallinity, and structural identification.
The D8 DISCOVER is an X-ray diffraction instrument, perfect for thin film application, equipped with four motorized axes stage, having as typical applications: XR Reflectometry, Rocking measurements, RSM measurements and structural phase identification. The equipment can works in two differents configurations, Bragg-Brentano and Parallel configuration.
The D8 Advance A25 is equipped by two different configurations, Bragg-Brentano geometry with electrochemical cell (Cu radiation) and Debye-Scherrer geometry (Mo radiation) with a Johansson monochromator for capillary measurements.
Powder Diffraction Software:
EVA – Phase identification and quantitative phase analysis
TOPAS – Profile analysis, quantitative analysis, structure analysis
Materials Research Software:
MULTEX –Texture analysis
LEPTOS – Thin film analysis/Residual stress
X-Ray Diffraction
Service
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
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This email address is being protected from spambots. You need JavaScript enabled to view it.
This email address is being protected from spambots. You need JavaScript enabled to view it.
By phone:
+34 935801853
Ext. 290
Scientist in charge:
The Nanoquim Platform also counts with a portable air particle counter. Vertex. Model 3415. It is an equipment that measures air quality in terms of the number of particles. This allows to know if the clean room keep the specifications class 10.000 or type ISO7.
Nanoquim
Platform
ICMAB
Campus UAB
(in front of Firehouse)
08193, Bellaterra
Spain
By email:
This email address is being protected from spambots. You need JavaScript enabled to view it.
By phone:
Luigi: 436164
Marta: 436165
Lab 1: 436151
Lab 2: 436152
Lab 3: 436153
Lab 4: 436154
Lab 5: 436155
SCIENTIFIC & TECHNICAL SERVICES
The Bioservice Platform is open to the different research groups working in the area of biomaterials. The service caries out biological studies, both with cells and with bacteria, of the new materials and devices developed
Technician
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Technician
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outside of the Biolab, room 2001
outside of the Biolab, room 2001
Outside of the Biolab, Nanobioelectronics and Biosensors Lab
To use the Bioservice and the different equipment, you should contact This email address is being protected from spambots. You need JavaScript enabled to view it. by mail. After a first meeting, in which the main details of the experiments to perform will be exposed, the Bioservice will prepare a budget. Once the budget is accepted, the work at the Bioservice can start, previously according the calendar and deadlines.
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41.5013,2.1116
Biolab Facility
ICN2 building
Universitat Autònoma de Barcelona Campus
Av. de Serragalliners, s/n
08193 Bellaterra
Barcelona
By email:
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The Bioservice Facility has received funds from the CENanoTech project (2015 FEDER/S-16). In turn, the CENanoTech project is funded through the call for unique institutional R&D infrastructures launched by the Universities and Research Secretariat of the Regional Ministry of Economy and Knowledge of the Government of Catalonia, with funding received from the European Regional Development Fund (ERDF) under the Operational Programme Catalonia 2014-2020. The project has also been co-funded by the Severo Ochoa Programme, granted by the back then Spanish Ministry of Economy and Competitiveness (SEV-2013-0295).
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Executive Assistant
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Direction
Institut de Ciència de Materials de Barcelona, ICMAB-CSIC
Carrer dels Til·lers s/n
Campus UAB
08193, Bellaterra
Catalunya, Spain
By email:
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By phone:
+34 935801853
Helmholtz Zentrum Berlin Mat & Energie GmbH
Germany
Laboratoire de Physico-Chimie, Pharmacotechnie et Biopharmacie
France
Technische Universität München, Physik Department
Germany
Applied Superconductivity Center, National High Magnetic Field Laboratory
USA
CIC biomaGUNE
Spain
University of Cambridge, Department of Materials Science & Metallurgy
UK
Università di Trieste1 and CIC biomaGUNE2
1Italy, 2Spain
Lehigh University
USA
School of Chemical & Biomolecular Engineering - Georgia Institute of Technology
USA
Collège de France, Chimie du solide et de l'énergie
France
Scuola Internazionale Superiore di Studi Avanzati (SISSA)
Italy
Director - W. M. Keck Smart Mat. Int. Lab.
USA
Scientific Advisory Board
Institut de Ciència de Materials de Barcelona, ICMAB-CSIC
Carrer dels Til·lers s/n
Campus UAB
08193, Bellaterra
Catalunya, Spain
By email:
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By phone:
+34 935801853
The Scientific Executive Board (SEB) is formed by the Direction team (Director and Deputy Directors), the members of the Severo Ochoa Strategic Managing Unit, and the coordinators of the 5 research lines (RL) of the Institute.
The SEB is in charge of taking decisions regarding the scientific strategy that the ICMAB follows. It also is in charge of deciding the strategic priority actions of the center and or organizing the Scientific Advisory Board (SAB) meeting, held once a year at ICMAB.
Scientific Executive Board
Institut de Ciència de Materials de Barcelona, ICMAB-CSIC
Carrer dels Til·lers s/n
Campus UAB
08193, Bellaterra
Catalunya, Spain
By email:
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By phone:
+34 935801853
The Institute Governing Board is the governing body formed by Direction (as President), Deputy Direction, General Manager (as Secretary), by one member of each Department and by the Staff representatives.
The Institute Governing Board meets twice per year and is in charge of taking some important decisions concerning the Institute.
Institute Governing Board
Institut de Ciència de Materials de Barcelona, ICMAB-CSIC
Carrer dels Til·lers s/n
Campus UAB
08193, Bellaterra
Catalunya, Spain
By email:
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By phone:
+34 935801853
The Scientific Board (el Claustre) is formed by the Direction team (Director and Deputy Directors), the General Manager and by all the permanent scientists (Research Professors, Research Scientists and Tenured Scientists) of the Institute.
Scientific Board
Institut de Ciència de Materials de Barcelona, ICMAB-CSIC
Carrer dels Til·lers s/n
Campus UAB
08193, Bellaterra
Catalunya, Spain
By email:
This email address is being protected from spambots. You need JavaScript enabled to view it.
By phone:
+34 935801853